5,7-二硝基喹啉-8-醇合成路线 （共 12 条）
反应条件
konz. wss. Salpetersaeure;
参考文献
Carboni
Gazzetta Chimica Italiana, 1955 , vol. 85, p. 1194,1198
反应条件
thionyl chloride in N,N-dimethyl-formamide; toluene
参考文献
Ilyina; Mel'Nikov; Luyksaar; Krayushkin; P'Yankov; Barachevsky; Fedyanin
Russian Chemical Bulletin, 2008 , vol. 57, # 7 p. 1444 - 1450
参考文献
Dikshoorn
Recueil des Travaux Chimiques des Pays-Bas, 1929 , vol. 48, p. 552
反应条件
nitric acid
T=40°C; 1 h;
参考文献
Clavier, Sylvain; Rist, ystein; Hansen, Stina; Gerlach, Lars-Ole; Hoegberg, Thomas; Bergman, Jan
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 23 p. 4248 - 4253
反应条件
nitric acid
T=50°C; 0.25 h;
参考文献
Sutter, Peter; Weis, Claus D.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 29 - 32
参考文献
Sutter, Peter; Weis, Claus D.
Journal of Heterocyclic Chemistry, 1986 , vol. 23, p. 29 - 32
反应条件
1: hydrochloric acid; glycerol; concentrated sulfuric acid
2: nitric acid
View Scheme
参考文献
Skraup
Monatshefte fuer Chemie, 1882 , vol. 3, p. 551
Monatshefte fuer Chemie, 1883 , vol. 4, p. 698
参考文献
Urbanski
Roczniki Chemii, 1951 , vol. 25, p. 297,305
Chem.Abstr., 1954 , p. 4546
参考文献
Airan; Wagle
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1954 , vol. 23/A, p. 29
反应条件
1: 78 percent / POCl3 / 2 h / Heating
2: 66 percent / Et3N / tetrahydrofuran / 12 h / Heating
View Scheme
参考文献
Clavier, Sylvain; Rist, ystein; Hansen, Stina; Gerlach, Lars-Ole; Hoegberg, Thomas; Bergman, Jan
Organic and Biomolecular Chemistry, 2003 , vol. 1, # 23 p. 4248 - 4253
