反应条件
Multi-step reaction with 3 steps 1: 87 percent / pyridine / 1) 0 to 5 deg C, 5.5 h; 2) 8 deg C, 12 h.2: 76 percent / p-toluenesulfonic acid / benzene / 4 h / Heating3: 78 percent / Li2CuCl4 / diethyl ether; tetrahydrofuran / 1) -70 deg C, 2h; 2) room temp., 12 h.
参考文献
Odinokov, V. N.; Akhmetova, V. R.; Ishmuratov, G. Yu.; Botsman, L. P.; Tolstikov, G. A. Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, # 5 p. 851 - 855Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 5 p. 953 - 957