反应条件
1: 1.) CuI*PBu3 / 1.) hexane, toluene, -40 deg C, 30 min; 2.) toluene, 30 min, -80 deg C -40 deg C, 16 h 2: 1.) LiOH*H2O; 2.) aq. HCl / 1.) THF, 65 deg C, 5 d View Scheme
参考文献
Oppolzer, Wolfgang; Kingma, Arend J.; Poli, Giovanni
Tetrahedron, 1989 , vol. 45, # 2 p. 479 - 488