1,3-双(4-氟苯甲酰)苯合成路线 (共 3 条)
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
反应条件
aluminium trichloride T=23°C; Friedel-Crafts acylation; 4 h;
参考文献
Zhao, Weili; Carreira, Erick M.
Organic Letters, 2006 , vol. 8, # 1 p. 99 - 102
反应条件
1: 3-amino-phenol With potassium carbonate in N,N-dimethyl-formamide; toluene Dean-Stark trapReflux; 2: 1,3-bis(4'-fluorobenzoyl)benzene in N,N-dimethyl-formamide; toluene T=130 - 150°C; Inert atmosphere;
参考文献
Journal of Polymer Science, Part A: Polymer Chemistry, , vol. 48, # 13 p. 2878 - 2884