二苄基 N,N-二异丙基亚磷酰胺合成路线 （共 19 条）
反应条件
triethylamine in diethyl ether T=20°C; 2 h;
参考文献
Tetrahedron, , vol. 47, # 26 p. 4709 - 4722
反应条件
1: diisopropylamine With phosphorus trichoride in hexane T=0°C; Inert atmosphereReflux; 2: benzyl alcohol With triethylamine in hexane T=0 - 20°C; Inert atmosphere;
参考文献
Amino Acids, , vol. 39, # 2 p. 367 - 373
反应条件
1: diisopropylamine With phosphorus trichoride in hexane T=0 - 20°C; 2: benzyl alcohol With triethylamine in diethyl ether; hexane T=20°C; 1 h;
参考文献
Organic and Biomolecular Chemistry, , vol. 11, # 34 p. 5702 - 5713
反应条件
N,N-diisopropylamine tetrazolide in dichloromethane 2 h;
参考文献
Helvetica Chimica Acta, , vol. 70, p. 175 - 186
反应条件
1: 6.3 g / PCl3 / diethyl ether / -10 - 20 °C 2: ethyl diisopropylamine / acetonitrile / -10 - 20 °C View Scheme
参考文献
Tetrahedron, , vol. 55, # 23 p. 7251 - 7270
反应条件
1: 78 percent / 2 M NaOH / toluene / 48 h / 25 °C 2: 1) diisopropylethylamine, 2) benzyl alcohol / 1) THF, 25 deg C, 18 h, 2) THF, 25 deg C, 4 h View Scheme
参考文献
Carbohydrate Research, , vol. 230, # 1 p. 63 - 78
反应条件
1: 95 percent / diethyl ether / 1 h, -10 degC, r.t., overnight 2: 78 percent / diisopropylammonium tetrazolide / CH2Cl2 / 2 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 70, p. 175 - 186
反应条件
1: 71 percent / PCl3, pyridine / diethyl ether / 1.5 h / -78 °C 2: 95 percent / diethyl ether / 1 h, -10 degC, r.t., overnight 3: 78 percent / diisopropylammonium tetrazolide / CH2Cl2 / 2 h View Scheme
参考文献
Helvetica Chimica Acta, , vol. 70, p. 175 - 186
反应条件
N-ethyl-N,N-diisopropylamine; benzyl alcohol 1) THF, 25 deg C, 18 h, 2) THF, 25 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 230, # 1 p. 63 - 78
反应条件
3-(benzyloxycarbonylamino)-1-propanol; N-ethyl-N,N-diisopropylamine 1) THF, 25 deg C, 18 h, 2) THF, 25 deg C, 4 h; Yield given. Multistep reaction;
参考文献
Carbohydrate Research, , vol. 230, # 1 p. 63 - 78
