[3-[(三甲基硅烷基)氧基]-2-环己烯-1-基]-苯合成路线 （共 10 条）
反应条件
ammonium cerium(IV) nitrate; toluene-4-sulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium carbonate 1.) MeOH, 20 deg C, 2.) C6H6, reflux, 3.0 h; Yield givenMultistep reaction;
参考文献
Belli Paolobelli, Anna; Ruzziconi, Renzo; Lupattelli, Paolo; Scafato, Patrizia; Spezzacatena, Caterina
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3364 - 3368
反应条件
copper(I) bromide in diethyl ether
T=-50 - -40°C; 0.25 h;
参考文献
Andringa; Oosterveld; Brandsma
Synthetic Communications, 1991 , vol. 21, # 12-13 p. 1393 - 1396
反应条件
copper(l) iodide; lithium chloride in tetrahydrofuran
T=0°C; 0.5 h;
参考文献
Reetz, Manfred T.; Kindler, Alois
Journal of Organometallic Chemistry, 1995 , vol. 502, # 1-2 p. C5 - C7
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=-78°C; 1 h;
参考文献
Johnson, Carl R.; Marren, Thomas J.
Tetrahedron Letters, 1987 , vol. 28, # 1 p. 27 - 30
反应条件
bis(acetylacetonate)nickel(II); manganese; 2,9-dimethyl-1,10-phenanthroline in N,N-dimethyl acetamide
T=20°C;
参考文献
Shrestha, Ruja; Dorn, Stephanie C. M.; Weix, Daniel J.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 751 - 762
反应条件
bis(acetylacetonate)nickel(II); manganese; 2,9-dimethyl-1,10-phenanthroline in N,N-dimethyl acetamide
T=20°C;
参考文献
Shrestha, Ruja; Dorn, Stephanie C. M.; Weix, Daniel J.
Journal of the American Chemical Society, 2013 , vol. 135, # 2 p. 751 - 762
反应条件
naphthalene; lithium; lithium bromide
1.) THF, -35 deg C, 15 min, 2.) THF, -78 deg C, 1.5 h; Yield given. Multistep reaction;
参考文献
Stack, Douglas E.; Dawson, Bryan T.; Rieke, Reuben D.
Journal of the American Chemical Society, 1991 , vol. 113, # 12 p. 4672 - 4673
反应条件
CuI*LiCl
Yield given;
参考文献
Belli Paolobelli, Anna; Ruzziconi, Renzo; Lupattelli, Paolo; Scafato, Patrizia; Spezzacatena, Caterina
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3364 - 3368
反应条件
ammonium cerium(IV) nitrate; sulfuric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; calcium carbonate
1.) MeOH, 20 deg C, 2.) C6H6, reflux, 2 h, 3.) MeOH, 24 h; Yield givenMultistep reaction;
参考文献
Belli Paolobelli, Anna; Ruzziconi, Renzo; Lupattelli, Paolo; Scafato, Patrizia; Spezzacatena, Caterina
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 3364 - 3368
反应条件
methanol; ammonium cerium(IV) nitrate; sulfuric acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone
1.) 20 deg C, 2.) methanol, 0 deg C, 240 min; Yield given. Multistep reaction;
参考文献
Ricci, Giacomo; Ruzziconi, Renzo
Journal of Organic Chemistry, 2005 , vol. 70, # 2 p. 611 - 623
