1: in tetrahydrofuran T=55°C; 8 h; Inert atmosphere; 2: With water; ammonium chloride in tetrahydrofuran Inert atmosphere;

sodium hydrogencarbonate in tetrahydrofuran T=0 - 20°C; 0.5 h;

1: 2-methylbenzoic chloride With pyridine; trimethylsilylazide in N,N-dimethyl-formamide T=20°C; Curtius rearrangement; Microflow reactionInert atmosphere; 2: benzyl alcohol With acetic acid in N,N-dimethyl-formamide T=110°C; Microflow reactionInert atmosphere;

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1: copper View Scheme

T=130 - 170°C; Rate constant;

T=130 - 170°C; Rate constant;