1-苄基-4-苯基-1,2,3-噻唑合成路线 （共 52 条）
反应条件
octanoic acid; C27H31AgNO3P in toluene
T=48°C; 20 h; Inert atmosphere;
参考文献
McNulty, James; Keskar, Kunal; Vemula, Ramesh
Chemistry - A European Journal, 2011 , vol. 17, # 52 p. 14727 - 14730
反应条件
1: tetrahydrofuran / 15 h / 20 °C / |Inert atmosphere
2: copper(l) iodide; N,N,N',N'',N''-pentamethyldiethylenetriamine / tetrahydrofuran / 0.33 h / 20 °C / |Inert atmosphere
3: palladium diacetate; triethylamine; methanol
View Scheme
参考文献
Stefani, Helio A.; Vasconcelos, Stanley N. S.; Manarin, Flavia; Leal, Daiana M.; Souza, Frederico B.; Madureira, Lucas Sousa; Zukerman-Schpector, Julio; Eberlin, Marcos N.; Godoi, Marla N.; De Souza Galaverna, Renan
European Journal of Organic Chemistry, 2013 , # 18 p. 3780 - 3785
反应条件
Cu(ClO4)2*6H2O; potassium iodide; TBTA in tetrahydrofuran
T=20°C; 3 h; Reagent/catalyst;
参考文献
Barsoum, David N.; Brassard, Christopher J.; Deeb, Jason H. A.; Okashah, Najeah; Sreenath, Kesavapillai; Simmons, J.Tyler; Zhu, Lei
Synthesis (Germany), 2013 , vol. 45, # 17 art. no. SS-2013-Z0238-FA, p. 2372 - 2386
反应条件
copper(l) iodide; ammonia; ascorbic acid powder
T=25°C; 10 h;
参考文献
Ji, Pengju; Atherton, John H.; Page, Michael I.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 39 p. 7965 - 7969
反应条件
1: diethylamine; 5 palladium-copper on carbon / methanol / 0.42 h / 120 °C / |Inert atmosphere; |Microwave irradiation
2: 0.17 h / 120 °C / |Microwave irradiation; |Inert atmosphere
View Scheme
参考文献
Rossy, Cybille; Majimel, Jerome; Delapierre, Mona Treguer; Fouquet, Eric; Felpin, Francois-Xavier
Journal of Organometallic Chemistry, 2014 , vol. 755, p. 78 - 85
反应条件
1: copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C
2: copper(l) iodide; potassium fluoride; silver carbonate; 1,10-phenanthroline / N,N-dimethyl-formamide / 100 °C
View Scheme
参考文献
Fu, Dan; Zhang, Jian; Cao, Song
Journal of Fluorine Chemistry, 2013 , vol. 156, p. 170 - 176
反应条件
Cu phenylacetylide; triethylamine in tetrahydrofuran
T=20°C; 15 h;
参考文献
Buckley, Benjamin R.; Dann, Sandra E.; Heaney, Harry
Chemistry - A European Journal, 2010 , vol. 16, # 21 p. 6278 - 6284
反应条件
1: copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C
2: potassium fluoride; silver carbonate; 1,10-phenanthroline / N,N-dimethyl-formamide / 100 °C
View Scheme
参考文献
Fu, Dan; Zhang, Jian; Cao, Song
Journal of Fluorine Chemistry, 2013 , vol. 156, p. 170 - 176
反应条件
1: potassium iodide; tert.-butylhydroperoxide / methanol / 20 °C
2: copper(l) iodide; triethylamine / tetrahydrofuran / 20 °C
3: potassium fluoride; silver carbonate; 1,10-phenanthroline / N,N-dimethyl-formamide / 100 °C
View Scheme
参考文献
Fu, Dan; Zhang, Jian; Cao, Song
Journal of Fluorine Chemistry, 2013 , vol. 156, p. 170 - 176
反应条件
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 24 h / Inert atmosphere; Reflux
2: pyridine; sodium azide; potassium carbonate; copper(II) sulfate; ascorbic acid powder / methanol; water
View Scheme
参考文献
Ladouceur, Sebastien; Soliman, Ahmed M.; Zysman-Colman, Eli
Synthesis, 2011 , # 22 art. no. M79111SS, p. 3604 - 3611
