2-氨基-N,N-二乙基-乙酰胺盐酸盐(1:1)合成路线 （共 6 条）
反应条件
hydrogenchloride in water; ethyl acetate T=0°C;
参考文献
Tsukube, Hiroshi; Noda, Yuki; Kataoka, Yumiko; Miyake, Hiroyuki; Shinoda, Satoshi; Kojima-Yuasa, Akiko; Nishida, Yoshitake; Matsui-Yuasa, Isao
Dalton Transactions, 2008 , # 30 p. 4038 - 4043
反应条件
sodium hydrogencarbonate in benzene
参考文献
Roehnert,H.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1960 , vol. 293, p. 573 - 576
反应条件
1: in methanol
T=20°C; 3 h; Inert atmosphere;
2: With sodium cyanoborohydride in methanol
T=0 - 20°C;
参考文献
Kataoka, Yumiko; Paul, Dharam; Miyake, Hiroyuki; Yaita, Tsuyoshi; Miyoshi, Eisaku; Mori, Hirotoshi; Tsukamoto, Shinya; Tatewaki, Hiroshi; Shinoda, Satoshi; Tsukube, Hiroshi
Chemistry - A European Journal, 2008 , vol. 14, # 17 p. 5258 - 5266
反应条件
sodium carbonate in acetonitrile
Reflux;
参考文献
Tsukube, Hiroshi; Noda, Yuki; Kataoka, Yumiko; Miyake, Hiroyuki; Shinoda, Satoshi; Kojima-Yuasa, Akiko; Nishida, Yoshitake; Matsui-Yuasa, Isao
Dalton Transactions, 2008 , # 30 p. 4038 - 4043
反应条件
potassium carbonate in acetonitrile
18 h; Inert atmosphereReflux;
参考文献
Kataoka, Yumiko; Paul, Dharam; Miyake, Hiroyuki; Yaita, Tsuyoshi; Miyoshi, Eisaku; Mori, Hirotoshi; Tsukamoto, Shinya; Tatewaki, Hiroshi; Shinoda, Satoshi; Tsukube, Hiroshi
Chemistry - A European Journal, 2008 , vol. 14, # 17 p. 5258 - 5266
反应条件
1: in methanol
T=20°C; 2.5 h;
2: With sodium cyanoborohydride in methanol
T=20°C; 72 h; Further stages.;
参考文献
Kataoka, Yumiko; Paul, Dharam; Miyake, Hiroyuki; Shinoda, Satoshi; Tsukube, Hiroshi
Dalton Transactions, 2007 , # 26 p. 2784 - 2791
