in neat (no solvent) byproducts: hydrogen; introduction of n-BuNH2*BH3 under N2 into flask; heating in an oil bath by slow raising the temp. to 120°C for 30 min; heating at this temp. for 1 h; heating at 200°C for 1 h; distn. in vac.;
Mikhailov, B. M.; Dorokhov, V. A.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1961 , p. 1346 - 1348
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Gmelin Handbook: B: B-Verb.4, 13.3.1, page 325 - 329
