1,2,3,4-四氢-2,7-萘啶合成路线 （共 5 条）
反应条件
palladium on activated charcoal; hydrogen; potassium acetate in methanol T=20°C; 24 h;
参考文献
SUNSHINE LAKE PHARMA CO., LTD.; ZHANG, Jiancun; ZHANG, Yingjun; ZHANG, Weihong; LIU, Bing; ZHANG, Jiquan; LIU, Jinlei; ZHANG, Lu
Patent: WO2013/71697 A1, 2013 ;
Location in patent: Paragraph 00361 ;
反应条件
methanol; Lindlar's catalyst Hydrogenation;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 6, p. 408,411
反应条件
1: trichlorophosphate / 24 h / 180 °C 2: potassium acetate; hydrogen; palladium on activated charcoal / methanol / 24 h / 20 °C View Scheme
反应条件
1.1: ethylamine / ethanol / 48 h / 20 °C 1.2: 0.17 h / 100 °C 2.1: trichlorophosphate / 24 h / 180 °C 3.1: potassium acetate; hydrogen; palladium on activated charcoal / methanol / 24 h / 20 °C View Scheme
反应条件
1: 4-(N,N-dimethlyamino)pyridine / acetonitrile / 0 - 20 °C
2: acetic acid; hydrogen; palladium(II) oxide hydrate / 80 °C
View Scheme
参考文献
SUNSHINE LAKE PHARMA CO., LTD.; ZHANG, Jiancun; ZHANG, Yingjun; ZHANG, Weihong; LIU, Bing; ZHANG, Jiquan; LIU, Jinlei; ZHANG, Lu
Patent: WO2013/71697 A1, 2013 ;
