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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
108789-40-8
合成路线
（共 10 条）
201230-82-2
+
31268-20-9
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
反应条件
tetrakis(triphenylphosphine) palladium(0); cesium fluoride in tetrahydrofuran T=60°C; Suzuki-Miyaura reaction; 3 h;
参考文献
Medio-Simon, Mercedes; Mollar, Cristian; Rodriguez, Nuria; Asensio, Gregorio
Organic Letters, 2005 , vol. 7, # 21 p. 4669 - 4672
31268-20-9
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
581-80-6
+
1193-82-4
甲基苯基亚砜
+
108789-40-8
反应条件
cesium fluoride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran Heating;
参考文献
Rodriguez, Nuria; Cuenca, Ana; Ramirez De Arellano, Carmen; Medio-Simon, Mercedes; Peine, Denissa; Asensio, Gregorio
Journal of Organic Chemistry, 2004 , vol. 69, # 23 p. 8070 - 8076
31268-20-9
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
108789-40-8
反应条件
bromobenzene; palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
6952-59-6
间溴苯腈
+
31268-20-9
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
反应条件
palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
28715-70-0
+
402-49-3
1-溴-三氟对二甲苯
→
反应条件
108789-40-8
反应条件
in nitromethane T=75°C; 10 h;
参考文献
Kersten, Mathias; Wenschuh, Eberhard
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 80, # 1-4 p. 81 - 84
→
反应条件
反应条件
palladium diacetate; cesium fluoride; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in tetrahydrofuran T=65°C; Suzuki-Miyaura reaction; 5 h; Inert atmosphere;
参考文献
Mollar, Cristian; Besora, Maria; Maseras, Feliu; Asensio, Gregorio; Medio-Simon, Mercedes
Chemistry - A European Journal, 2010 , vol. 16, # 45 p. 13390 - 13397
1193-82-4
甲基苯基亚砜
→
反应条件
108789-40-8
反应条件
1: 80 percent / Br2; pyridine / acetonitrile / -40 - 20 °C 2: 23 percent / CsF; Pd(PPh3)4 / tetrahydrofuran / 3 h / 60 °C View Scheme
参考文献
Medio-Simon, Mercedes; Mollar, Cristian; Rodriguez, Nuria; Asensio, Gregorio
Organic Letters, 2005 , vol. 7, # 21 p. 4669 - 4672
30932-37-7
→
反应条件
108789-40-8
反应条件
sodium periodate in methanol; water 40 h; Ambient temperature;
参考文献
Renaud, Philippe; Bourquard, Thierry; Carrupt, Pierre-Alain; Gerster, Michele
Helvetica Chimica Acta, 1998 , vol. 81, # 6 p. 1048 - 1063
108-98-5
硫酚
→
反应条件
108789-40-8
反应条件
1: 96 percent / NaOH, Bu4NI / benzene; H2O / 24 h / Ambient temperature 2: 28 percent / NaIO4 / methanol; H2O / 40 h / Ambient temperature View Scheme
参考文献
Renaud, Philippe; Bourquard, Thierry; Carrupt, Pierre-Alain; Gerster, Michele
Helvetica Chimica Acta, 1998 , vol. 81, # 6 p. 1048 - 1063
402-49-3
1-溴-三氟对二甲苯
→
反应条件
108789-40-8
反应条件
1: 96 percent / NaOH, Bu4NI / benzene; H2O / 24 h / Ambient temperature 2: 28 percent / NaIO4 / methanol; H2O / 40 h / Ambient temperature View Scheme
参考文献
Renaud, Philippe; Bourquard, Thierry; Carrupt, Pierre-Alain; Gerster, Michele
Helvetica Chimica Acta, 1998 , vol. 81, # 6 p. 1048 - 1063
