(3-丁烯-1-基氧基)(二甲基)(2-甲基-2-丙基)硅烷合成路线 （共 18 条）
反应条件
1H-imidazole in N,N-dimethyl-formamide T=20°C; 48 h; Inert atmosphere;
参考文献
Ghosh, Arun K.; Li, Jianfeng
Organic Letters, 2009 , vol. 11, # 18 p. 4164 - 4167
反应条件
hydrogen; N1-(2-Amino-ethyl)-ethane-1,2-diamine in methanol T=25°C; 6 h;
参考文献
Yabe, Yuki; Yamada, Tsuyoshi; Nagata, Saori; Sawama, Yoshinari; Monguchi, Yasunari; Sajiki, Hironao
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 7 p. 1264 - 1268
反应条件
C29H40ClCuN2; sodium t-butanolate; tert-butyl alcohol in tetrahydrofuran; hexane T=40°C; 20 h; Inert atmosphere; chemoselective reaction;
参考文献
Semba, Kazuhiko; Fujihara, Tetsuaki; Xu, Tinghua; Terao, Jun; Tsuji, Yasushi
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1542 - 1550
反应条件
1: 1H-imidazole / N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere 2: C29H40ClCuN2; sodium t-butanolate; tert-butyl alcohol / tetrahydrofuran; hexane / 20 h / 40 °C / Inert atmosphere View Scheme
参考文献
Semba, Kazuhiko; Fujihara, Tetsuaki; Xu, Tinghua; Terao, Jun; Tsuji, Yasushi
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 8 p. 1542 - 1550
参考文献
Buswell, Marina; Fleming, Ian; Ghosh, Usha; Mack, Stephen; Russell, Matthew; Clark, Barry P.
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 20 p. 3006 - 3017
反应条件
1: With ozone in dichloromethane T=-78°C; 0.166667 h; 2: With triphenylphosphine on polystyrene in dichloromethane T=20°C; 14 h;
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Brown, Dearg S.; Baxendale, Ian R.; Ley, Steven V.
Chemistry - A European Journal, 2004 , vol. 10, # 10 p. 2529 - 2547
反应条件
1: With ozone in dichloromethane T=-78°C; 0.333333 h; 2: With diphenylphosphinopolystyrene in dichloromethane T=-78 - 20°C; 12 h;
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Ley, Steven V.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 22 p. 2521 - 2525
反应条件
dimethylsulfide; ozone 1.) CH2Cl2, -35 deg.C, 2.) CH2Cl2, 3h, RT; Yield given. Multistep reaction;
参考文献
Pirrung, Michael C.; Webster, Nicholas J. G.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3603 - 3613
反应条件
Mo(CHCMe2Ph)(NAr)lt;OCMe(CF3)2gt;2 (Schrock's molybdenum catalyst) in ethylene glycol dimethyl ether 4 h; Yields of byproduct given;
参考文献
Crowe, William E.; Goldberg, Daniel R.; Zhang, Zhijia J.
Tetrahedron Letters, 1996 , vol. 37, # 13 p. 2117 - 2120
反应条件
1.1: O3 / CH2Cl2 / 0.17 h / -78 °C 1.2: 93 percent / polymer-supported triphenylphosphine / CH2Cl2 / 14 h / 20 °C 2.1: N-tosyl-D-phenylalanine; BH3*THF / tetrahydrofuran; CH2Cl2 / 1.5 h / -96 - -78 °C View Scheme
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Ley, Steven V.
Angewandte Chemie - International Edition, 2003 , vol. 42, # 22 p. 2521 - 2525
