2-(3-溴丙基)-5,5-二甲基-1,3-二噁烷合成路线 (共 2 条)
反应条件
toluene-4-sulfonic acid in phosphorus tribromide; 1,2-dichloro-ethane
参考文献
Bartels; Gunter
Patent: US4847391 A1, 1989 ;
反应条件
n-butyllithium; potassium tert-butylate
1.) pentane, 22 h, 22 deg C, 2.) 0 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bock, Klaus; Skrydstrup, Troels
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 5 p. 1181 - 1186