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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
108835-16-1
合成路线
(共 10 条)
108835-16-1
→
反应条件
24300-91-2
2,7-二叔丁基芘
反应条件
1: 85 percent / I2 / benzene / 6 h / 60 °C 2: 75 percent / DDQ / benzene / 4 h / Heating View Scheme
参考文献
Tashiro, Masashi; Yamato, Takehiko; Kobayashi, Kazumasa; Arimura, Takashi
Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3196 - 3199
108835-16-1
→
反应条件
69080-03-1
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide in acetic acid 0.0833333 h; Ambient temperature;
参考文献
Yamato, Takehiko; Ide, Seiji; Tokuhisa, Kiwamu; Tashiro, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 271 - 275
108835-16-1
→
反应条件
69080-03-1
+
118249-39-1
反应条件
nitric acid; acetic acid 1 h; Ambient temperature;
参考文献
Tashiro, Masashi; Mataka, Shuntaro; Takezaki, Yoshinori; Takeshita, Michinori; Arimura, Takashi; et al.
Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 451 - 458
108835-16-1
→
反应条件
69080-03-1
反应条件
chloro-trimethyl-silane; sodium iodide in dichloromethane; acetonitrile 24 h; Ambient temperature;
参考文献
Yamato, Takehiko; Matsumoto, Jun-ichi; Tashiro, Masashi
Journal of Chemical Research, Miniprint, 1994 , # 7 p. 1401 - 1410
71-23-8
丙醇
+
108835-16-1
→
反应条件
69080-03-1
+
137594-41-3
+
137594-45-7
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide 0.0833333 h; Ambient temperature;
参考文献
Yamato, Takehiko; Ide, Seiji; Tokuhisa, Kiwamu; Tashiro, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 271 - 275
64-17-5
乙醇
+
108835-16-1
→
反应条件
69080-03-1
+
137594-40-2
+
137594-44-6
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide 0.0833333 h; Ambient temperature;
参考文献
Yamato, Takehiko; Ide, Seiji; Tokuhisa, Kiwamu; Tashiro, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 271 - 275
67-56-1
甲醇
+
108835-16-1
→
反应条件
69080-03-1
+
137594-39-9
+
137594-43-5
反应条件
N,N,N-trimethyl-1-phenylmethanaminium tribromide 0.0833333 h; Ambient temperatureother 8-methoxy<2.2>metacyclophanes, various alcohol; also without alcohols, other amounts of reagent; Product distributionMechanism;
参考文献
Yamato, Takehiko; Ide, Seiji; Tokuhisa, Kiwamu; Tashiro, Masashi
Journal of Organic Chemistry, 1992 , vol. 57, # 1 p. 271 - 275
108835-11-6
→
反应条件
108835-16-1
反应条件
T=500°C; P=2 - 3 Torr;
参考文献
Tashiro, Masashi; Yamato, Takehiko; Kobayashi, Kazumasa; Arimura, Takashi Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3196 - 3199
108835-06-9
→
反应条件
108835-16-1
反应条件
Multi-step reaction with 2 steps 1: 98 percent / m-chloroperbenzoic acid / CHCl3 / 48 h / Ambient temperature2: 85 percent / 500 °C / 2 - 3 Torr
参考文献
Tashiro, Masashi; Yamato, Takehiko; Kobayashi, Kazumasa; Arimura, Takashi Journal of Organic Chemistry, 1987 , vol. 52, # 15 p. 3196 - 3199
108835-16-1
→
反应条件
118249-39-1
反应条件
With nitric acid; acetic acid 1 h; Ambient temperature;
参考文献
Tashiro, Masashi; Mataka, Shuntaro; Takezaki, Yoshinori; Takeshita, Michinori; Arimura, Takashi; et al. Journal of Organic Chemistry, 1989 , vol. 54, # 2 p. 451 - 458