反应条件
butyllithium; diisopropylamine in tetrahydrofuran; hexane
soln. of BuLi in hexane added to soln. of (iPr)2NH in THF at 0°C,stirred for 20 min, cooled to -78°C, soln. of Ph3SnH in THF adde d, stirred for 1 h, warmed to -10°C, CH3I added, heated at 45°C for 1 h; cooled to ambient temp., aq. NH4Cl added, extracted with diethyl ether, combined org. phases dried over MgSO4, filtered, concd. under vac.; elem. anal.;
参考文献
Helliwell, Madeleine; Thomas, Eric J.; Townsend, Linda A.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 10 p. 1286 - 1296
