methanesulfonic acid in toluene 0.333333 h; Heating;
参考文献
Bierer, Donald E.; O'Connell, John F.; Parquette, Jon R.; Thompson, Charles M.; Rapoport, Henry
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1390 - 1405
1: 1) LDA / 1) THF, hexanes, -78 deg C, 2) -19 to -15 deg C
2: 79 percent / NaBH4 / tetrahydrofuran; propan-2-ol / a) 0 deg C to room temperature, overnight, b) 0 deg C to room temperature, 8 h
View Scheme
参考文献
Bierer, Donald E.; O'Connell, John F.; Parquette, Jon R.; Thompson, Charles M.; Rapoport, Henry
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1390 - 1405
1: 1) LDA / 1) THF, hexanes, -78 deg C, 2) -19 to -15 deg C
2: 79 percent / NaBH4 / tetrahydrofuran; propan-2-ol / a) 0 deg C to room temperature, overnight, b) 0 deg C to room temperature, 8 h
View Scheme
参考文献
Bierer, Donald E.; O'Connell, John F.; Parquette, Jon R.; Thompson, Charles M.; Rapoport, Henry
Journal of Organic Chemistry, 1992 , vol. 57, # 5 p. 1390 - 1405
