hydrogenchloride in 1,4-dioxane; water; ethyl acetate 0.5 h; Product distribution / selectivity;

1: 70.2 percent / dimethylsulfoxide / 3 h / 90 °C 2: 1) 100percent sulfuric acid, lithium aluminium hydride / tetrahydrofuran / 2 h / below 40 deg C 3: 52.5 percent / ethanol; tetrahydrofuran / 14 h View Scheme

1: 1) 100percent sulfuric acid, lithium aluminium hydride / tetrahydrofuran / 2 h / below 40 deg C 2: 52.5 percent / ethanol; tetrahydrofuran / 14 h View Scheme

1: 52.5 percent / ethanol; tetrahydrofuran / 14 h View Scheme

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