4’-羟基-3,3’,5-三甲氧基二苯乙烯合成路线 （共 4 条）
反应条件
boron tribromide; isoascorbic acid in dichloromethane T=-78 - 20°C; Inert atmosphere;
参考文献
Lee, Hyun Suck; Lee, Byung Won; Kim, Mi Ran; Jun, Jong-Gab
Bulletin of the Korean Chemical Society, 2010 , vol. 31, # 4 p. 971 - 975
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -78 °C 1.2: 35 percent / tetrahydrofuran; hexane / 20 °C 2.1: 88 percent / TBAF / tetrahydrofuran / 0.75 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 16 p. 3546 - 3554
反应条件
1.1: n-BuLi / tetrahydrofuran; hexane / 2 h / -78 °C 1.2: 35 percent / tetrahydrofuran; hexane / 20 °C 2.1: 88 percent / TBAF / tetrahydrofuran / 0.75 h View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 46, # 16 p. 3546 - 3554
反应条件
in sulfuric acid; acetone 4 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 36, p. 1545 - 1549
