二乙基 3,5-二甲氧基苄基磷酸酯合成路线 （共 23 条）
反应条件
T=130°C; Michaelis-Arbuzov reaction; 4 h; Inert atmosphere;
参考文献
Tetrahedron Letters, , vol. 53, # 27 p. 3521 - 3523
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 2 p. 883 - 892
反应条件
Esterification; Arbusov reaction;
参考文献
Tetrahedron Letters, , vol. 41, # 29 p. 5475 - 5478
反应条件
iodine T=150°C; 3 h;
参考文献
Journal of Organometallic Chemistry, , vol. 691, # 12 p. 2785 - 2792
反应条件
1: 94.4 percent / SOCl2 / diethyl ether / 3 h / 20 °C 2: 4 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 53, # 12 p. 1587 - 1590
反应条件
T=130°C; Michaelis-Arbuzov rearrangement; 24 h;
参考文献
Bioorganic and Medicinal Chemistry, , vol. 12, # 21 p. 5571 - 5578
反应条件
1: 92.3 percent / LiAlH4 / diethyl ether / 4 h / Heating 2: 94.4 percent / SOCl2 / diethyl ether / 3 h / 20 °C 3: 4 h / Heating View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 53, # 12 p. 1587 - 1590
反应条件
1: SOCl2 2: 92 percent / LiAlH4 / diethyl ether 3: 94 percent / PBr3 / CH2Cl2 4: 95 percent / 130 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 47, # 3 p. 167 - 174
反应条件
1: NaOH 2: SOCl2 3: 92 percent / LiAlH4 / diethyl ether 4: 94 percent / PBr3 / CH2Cl2 5: 95 percent / 130 °C View Scheme
参考文献
Journal of Labelled Compounds and Radiopharmaceuticals, , vol. 47, # 3 p. 167 - 174
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 3 h / 20 °C / |Inert atmosphere 2: hydrogenchloride / water / |Inert atmosphere 3: 10 h / 140 °C / |Inert atmosphere View Scheme
参考文献
Synthetic Communications, , vol. 42, # 24 p. 3589 - 3597,9
Synthetic Communications, , vol. 42, # 24 p. 3589 - 3597
