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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻溴吡啶
合成路线
（共 1098 条）
109-04-6
邻溴吡啶
+
143-66-8
四苯硼钠
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
palladium diacetate; sodium carbonate in various solvent(s) Suzuki reaction; 0.2 h; microwave irradiation;
参考文献
Villemin, Didier; Gomez-Escalonilla, Maria Jose; Saint-Clair, Jean-Francois
Tetrahedron Letters, 2001 , vol. 42, # 4 p. 635 - 637
109-04-6
邻溴吡啶
+
2633-57-0
(三-2-丙烯-1-基硅烷基)-苯
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide T=80°C; 23 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
109-04-6
邻溴吡啶
+
100-58-3
溴化苯基镁
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1: phenyl-magnesium bromide With titanium tetraethoxide in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: 2-bromo-pyridine With tributylphosphine; cobalt(II) chloride in tetrahydrofuran T=20°C; Inert atmosphere; chemoselective reaction;
参考文献
Zeng, Jing; Liu, Kun Ming; Duan, Xin Fang
Organic Letters, 2013 , vol. 15, # 20 p. 5342 - 5345
109-04-6
邻溴吡啶
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
potassium carbonate; copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in tetrahydrofuran; N,N-dimethyl-formamide T=75°C; 23 h; Product distribution / selectivity;
参考文献
US2009/69577 A1, ;
Page/Page column 25-26 ;
109-04-6
邻溴吡啶
+
960-16-7
三丁基苯基锡
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; cesium fluoride; 3-tert-butyl-5-methyl-1-(2-(diphenylphosphino)phenyl)-1H-pyrazole in toluene T=60°C; Stille coupling; 10 h; Inert atmosphere;
参考文献
Pal, Anwesha; Ghosh, Raju; Adarsh; Sarkar, Amitabha
Tetrahedron, 2010 , vol. 66, # 29 p. 5451 - 5458
109-04-6
邻溴吡啶
+
100-59-4
苯基氯化镁
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran T=25°C; 5 h;
参考文献
Bonnet, Veronique; Mongin, Florence; Trecourt, Francois; Queguiner, Guy; Knochel, Paul
Tetrahedron, 2002 , vol. 58, # 22 p. 4429 - 4438
109-04-6
邻溴吡啶
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
1-methyl-pyrrolidin-2-one; tetrakis(triphenylphosphine) palladium(0) T=80°C; 6 h;
参考文献
Shimada, Shigeru; Yamazaki, Osamu; Tanaka, Toshifumi; Rao, Maddali L. N.; Suzuki, Yohichi; Tanaka, Masato
Angewandte Chemie - International Edition, 2003 , vol. 42, # 16 p. 1845 - 1848
109-04-6
邻溴吡啶
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
potassium carbonate; palladium diacetate in water; toluene
参考文献
Suzuki, Ken; Kobayashi, Tohru; Nishikawa, Takenobu; Hori, Yoji; Hagiwara, Toshimitsu
Patent: US2002/58837 A1, 2002 ;
109-04-6
邻溴吡啶
+
1352708-09-8
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium carbonate in ethanol T=100°C; Suzuki Coupling; 18 h; Inert atmosphere; Reagent/catalystSolvent;
参考文献
Goggins, Sean; Rosevere, Eleanor; Bellini, Clement; Allen, Joseph C.; Marsh, Barrie J.; Mahon, Mary F.; Frost, Christopher G.
Organic and Biomolecular Chemistry, 2014 , vol. 12, # 1 p. 47 - 52
109-04-6
邻溴吡啶
+
71478-47-2
→
反应条件
1008-89-5
2-苯基吡啶
反应条件
bis-triphenylphosphine-palladium(II) chloride in tetrahydrofuran; ethylene glycol dimethyl ether T=0 - 20°C; 0.5 h;
参考文献
Riguet, Eric; Alami, Mouad; Cahiez, Gerard
Tetrahedron Letters, 1997 , vol. 38, # 25 p. 4397 - 4400
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