Sakamoto, Takao; Kondo, Yoshinori; Takazawa, Nobuo; Yamanaka, Hiroshi
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 16 p. 1927 - 1934
n-butyllithium in tetrahydrofuran; diethyl ether; hexane under N2, n-BuLi in hexane cooled to -78°C, dild. with Et2O, ethereal soln. of heterocycle added dropwise with stirring, stirred for a while, after addn. of soln. of Me3SnCl in THF allowed to warm to room temp.; concd. in vac., methylcyclohexane added, filtered, fractionally distd.;elem. anal.;
参考文献
Jutzi, Peter; Gilge, Ullrich
Journal of Organometallic Chemistry, 1983 , vol. 246, # 2 p. 163 - 168