反应条件
1: copper / N,N-dimethyl-formamide / 9 h / 51 °C / |Inert atmosphere; |Large scale 2: sodium tetrahydroborate / ethanol / 2.5 h / 15 - 30 °C / |Inert atmosphere; |Large scale 3: pyridine / acetonitrile / 1.25 h / 10 - 18 °C / |Inert atmosphere; |Large scale 4: ammonia / water / 17 h / 20 - 25 °C / |Inert atmosphere View Scheme
参考文献
Ashwood, Michael S.; Alabaster, Ramon J.; Cottrell, Ian F.; Cowden, Cameron J.; Davies, Antony J.; Dolling, Ulf H.; Emerson, Khateeta M.; Gibb, Andrew D.; Hands, David; Wallace, Debra J.; Wilson, Robert D.
Organic Process Research and Development, 2004 , vol. 8, # 2 p. 192 - 200
