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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
邻溴吡啶
合成路线
（共 1098 条）
853955-69-8
+
109-04-6
邻溴吡啶
→
反应条件
1008-89-5
2-苯基吡啶
+
321903-29-1
1,3-二氢-1,1-二甲基-2,1-苯并氧硅杂环戊二烯
反应条件
copper(l) iodide; bis(η3-allyl-μ-chloropalladium(II)); potassium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in tetrahydrofuran; N,N-dimethyl-formamide T=75°C; 22 h; Inert atmosphere;
参考文献
Chen, Jinshui; Tanaka, Masaaki; Sahoo, Akhila K.; Takeda, Masahide; Yada, Akira; Nakao, Yoshiaki; Hiyama, Tamejiro
Bulletin of the Chemical Society of Japan, 2010 , vol. 83, # 5 p. 554 - 569
109-04-6
邻溴吡啶
+
338945-22-5
→
反应条件
1257204-53-7
+
202925-92-6
2-甲基-2-丙基4-戊烯-1-基氨基甲酸酯
反应条件
1: 2-bromo-pyridine With dicyclohexyl(2′,6′-dimethoxybiphenyl-2-yl)phosphine; tris-(dibenzylideneacetone)dipalladium(0); iodine; zinc in N,N-dimethyl-formamide T=0°C; Negishi coupling reaction; Inert atmosphere; 2: (S)-N-Boc-2-(iodomethyl)pyrrolidine in N,N-dimethyl-formamide T=0 - 20°C; Negishi coupling reaction; Inert atmosphere;
参考文献
Massah, Ahmad Reza; Ross, Andrew J.; Jackson, Richard F. W.
Journal of Organic Chemistry, 2010 , vol. 75, # 23 p. 8275 - 8278
109-04-6
邻溴吡啶
+
128796-39-4
4-三氟甲基苯硼酸
→
反应条件
203065-88-7
2-[4-(三氟甲基)苯基]吡啶
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in tetrahydrofuran; water T=70°C; 24 h;
参考文献
Xu, Qiu-Lei; Wang, Cheng-Cheng; Li, Tian-Yi; Teng, Ming-Yu; Zhang, Song; Jing, Yi-Ming; Yang, Xu; Li, Wei-Nan; Lin, Chen; Zheng, You-Xuan; Zuo, Jing-Lin; You, Xiao-Zeng
Inorganic Chemistry, 2013 , vol. 52, # 9 p. 4916 - 4925
109-04-6
邻溴吡啶
+
402-43-7
→
反应条件
203065-88-7
2-[4-(三氟甲基)苯基]吡啶
反应条件
manganese; NiBr2(2,2'-bipyridine); trifluoroacetic acid in N,N-dimethyl-formamide T=20°C; 1 h;
参考文献
Gosmini, Corinne; Bassene-Ernst, Carine; Durandetti, Muriel
Tetrahedron, 2009 , vol. 65, # 31 p. 6141 - 6146
109-04-6
邻溴吡啶
+
98-56-6
→
反应条件
203065-88-7
2-[4-(三氟甲基)苯基]吡啶
反应条件
1: 1-chloro-4-(trifluoromethyl)benzene With 3-chloroprop-1-ene; trifluoroacetic acid; zinc; Co(2,2'-bipyridine)Br2 in pyridine; N-dodecane; acetonitrile T=50°C; 2: 2-bromo-pyridine With bis-triphenylphosphine-palladium(II) chloride in pyridine; N-dodecane; acetonitrile T=50°C; Negishi coupling;
参考文献
Kazmierski, Igor; Gosmini, Corinne; Paris, Jean-Marc; Perichon, Jacques
Synlett, 2006 , # 6 p. 881 - 884
109-04-6
邻溴吡啶
+
402-51-7
→
反应条件
203065-88-7
2-[4-(三氟甲基)苯基]吡啶
反应条件
nickel Inert atmosphere;
参考文献
Gao, Ke; Lee, Pin-Sheng; Fujita, Takeshi; Yoshikai, Naohiko
Journal of the American Chemical Society, 2010 , vol. 132, # 35 p. 12249 - 12251
109-04-6
邻溴吡啶
+
5350-57-2
→
反应条件
19848-68-1
反应条件
2,2'-bis-(diphenylphosphino)-1,1'- binaphthyl; sodium t-butanolate; palladium diacetate in toluene T=100°C; 8 h;
参考文献
Arterburn; Rao; Ramdas; Dible
Organic letters, 2001 , vol. 3, # 9 p. 1351 - 1354
109-04-6
邻溴吡啶
→
反应条件
694-85-9
+
19006-63-4
反应条件
1: sodium hydride 2: 0.08 h / Microwave irradiation View Scheme
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
109-04-6
邻溴吡啶
→
反应条件
19006-63-4
反应条件
1: sodium hydride 2: 0.08 h / 150 °C / Microwave irradiation View Scheme
参考文献
Iida, Hirokazu; Suda, Machiko; Nakajima, Etsuko; Hakamatsuka, Hiroko; Nagashima, Yuka; Joho, Kouta; Amemiya, Kenta; Moromizato, Tatsuya; Matsumoto, Kiyoshi; Murakami, Yasuoki; Hamana, Hiroshi
Heterocycles, 2010 , vol. 81, # 9 p. 2057 - 2062
109-04-6
邻溴吡啶
+
119-61-9
→
反应条件
19490-90-5
反应条件
tert.-butyl lithium in tetrahydrofuran; pentane T=-78 - 20°C; 6 h; diastereoselective reaction;
参考文献
Goto, Sachio; Velder, Janna; El Sheikh, Sherif; Sakamoto, Yuki; Mitani, Masatoshi; Elmas, Said; Adler, Andreas; Becker, Anne; Neudoerfl, Joerg-Martin; Lex, Johann; Schmalz, Hans-Guenther
Synlett, 2008 , # 9 p. 1361 - 1365
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