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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲基吡啶
合成路线
（共 842 条）
109-06-8
2-甲基吡啶
→
反应条件
4916-40-9
+
128802-88-0
+
130788-66-8
+
130788-67-9
+
130788-68-0
+
1437-15-6
1,2-双吡啶基乙烯
反应条件
sulfur 48 h; Heatingfurther indentificated products isolated; Product distribution;
参考文献
Gleich, Edward; Warnke, Zydmunt
Phosphorus, Sulfur and Silicon and the Related Elements, 1990 , vol. 53, # 1-4 p. 211 - 222
109-06-8
2-甲基吡啶
+
13716-10-4
二叔丁基氯化膦
→
反应条件
494199-72-3
反应条件
1: 2-picoline With lithium diisopropyl amide in diethyl ether T=-78 - 0°C; 1.08333 h; 2: chlorodi-tert-butylphosphine in diethyl ether T=-78 - 20°C;
参考文献
Zhang, Lei; Peng, Dongjie; Leng, Xuebing; Huang, Zheng
Angewandte Chemie - International Edition, 2013 , vol. 52, # 13 p. 3676 - 3680
Angew. Chem., 2013 , vol. 52, # 13 p. 3676 - 3680,5
109-06-8
2-甲基吡啶
→
反应条件
49618-59-9
反应条件
1: potassium carbonate / water / 0.02 h / 100 °C / Microwave irradiation 2: water / Microwave irradiation 3: oxygen / water / Microwave irradiation View Scheme
参考文献
Gogoi, Shyamalee; Dutta, Mandakini; Gogoi, Junali; Boruah, Romesh Chandra
Tetrahedron Letters, 2011 , vol. 52, # 7 p. 813 - 816
109-06-8
2-甲基吡啶
+
50-00-0
甲醛
→
反应条件
49745-42-8
2-(2-吡啶)-1,3-丙二醇
反应条件
T=130 - 140°C;
参考文献
Guanti, Giuseppe; Narisano, Enrica; Riva, Renata
Tetrahedron Asymmetry, 1997 , vol. 8, # 13 p. 2175 - 2187
109-06-8
2-甲基吡啶
+
50-00-0
甲醛
→
反应条件
103-74-2
2-羟乙基吡啶
+
49745-42-8
2-(2-吡啶)-1,3-丙二醇
反应条件
potassium hydroxide; water T=130 - 136°C; P=7355.08 Torr;
参考文献
Ohki; Noike
Yakugaku Zasshi, 1952 , vol. 72, p. 490
Chem.Abstr., 1953 , p. 6418
Full Text Show Details
Shono et al.
Kogyo Kagaku Zasshi, 1954 , vol. 57, p. 902
Chem.Abstr., 1956 , p. 999
109-06-8
2-甲基吡啶
→
反应条件
501948-05-6
罗沙布林
反应条件
1.1: bromine / ethyl acetate / 1 h / 20 °C 1.2: 2.5 h / 0 - 20 °C 2.1: N,N-dimethyl-formamide; dimethyl sulfate / N,N-dimethyl-formamide / 0.25 h / 20 °C / |Inert atmosphere 2.2: |Inert atmosphere 3.1: borane-THF / acetonitrile; methanol / 1 h / 50 °C 4.1: tetrahydrofuran / -50 - -40 °C / |Inert atmosphere 5.1: 4-(N,N-dimethlyamino)pyridine; triethylamine / tetrahydrofuran / 2 h / -30 - -25 °C / |Inert atmosphere View Scheme
参考文献
Li, Hao; Xia, Zhiqiang; Chen, Shoujun; Koya, Keizo; Ono, Mitsunori; Sun, Lijun
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 246 - 250
109-06-8
2-甲基吡啶
→
反应条件
501948-42-1
反应条件
1.1: bromine / ethyl acetate / 1 h / 20 °C 1.2: 2.5 h / 0 - 20 °C 2.1: N,N-dimethyl-formamide; dimethyl sulfate / N,N-dimethyl-formamide / 0.25 h / 20 °C / |Inert atmosphere 2.2: |Inert atmosphere View Scheme
参考文献
Li, Hao; Xia, Zhiqiang; Chen, Shoujun; Koya, Keizo; Ono, Mitsunori; Sun, Lijun
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 246 - 250
109-06-8
2-甲基吡啶
→
反应条件
501948-43-2
反应条件
1.1: bromine / ethyl acetate / 1 h / 20 °C 1.2: 2.5 h / 0 - 20 °C 2.1: N,N-dimethyl-formamide; dimethyl sulfate / N,N-dimethyl-formamide / 0.25 h / 20 °C / |Inert atmosphere 2.2: |Inert atmosphere 3.1: borane-THF / acetonitrile; methanol / 1 h / 50 °C View Scheme
参考文献
Li, Hao; Xia, Zhiqiang; Chen, Shoujun; Koya, Keizo; Ono, Mitsunori; Sun, Lijun
Organic Process Research and Development, 2007 , vol. 11, # 2 p. 246 - 250
109-06-8
2-甲基吡啶
+
552-89-6
邻硝基苯甲醛
→
反应条件
50385-24-5
反应条件
acetic anhydride 27 h; Inert atmosphereReflux;
参考文献
VENTRUS BIOSCIENCES, INC.; AMER, Moh, Samir
Patent: WO2013/70236 A1, 2013 ;
Location in patent: Page/Page column 13 ;
109-06-8
2-甲基吡啶
→
反应条件
50385-28-9
2-[2-(2-吡啶基)乙基]苯胺
反应条件
1: 175 °C 2: aqueous HI; red phosphorus / 160 °C View Scheme
参考文献
Shaw; Wagstaff
Journal of the Chemical Society, 1933 , p. 77
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