1: alpha-chloropyridine With lithium diisopropyl amide in tetrahydrofuran; hexane T=-78°C; 2.33333 h; 2: boric acid trimethyl ester in tetrahydrofuran; hexane T=-78°C; 2.33333 h; 3: With hydrogenchloride in water pH=~ 4;
参考文献
Koei Chemical Co., Ltd.
Patent: EP1460079 A1, 2004 ;
Location in patent: Page 5-6 ;
1: With lithium diisopropyl amide in diethyl ether T=-60°C; 0.75 h; 2: With tri-isopropoxy-borane in diethyl ether T=-60 - 20°C; 3: With sodium hydroxide in diethyl ether T=20°C;
iodine; fluorine; triethylamine in 1,2,2-trifluoro-trichloroethane T=0°C;
参考文献
Chambers, Richard D.; Parsons, Mandy; Sandford, Graham; Skinner, Christopher J.; Atherton, Malcolm J.; Moilliet, John S.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 7 p. 803 - 810
lithium diisopropyl amide in tetrahydrofuran T=-70°C;
参考文献
Jeff Thrasher; Hembre, Erik J.; Gardinier, Kevin M.; Savin, Kenneth A.; Hong, Jian Eric; Jungheim, Louis N.
Heterocycles, 2006 , vol. 67, # 2 p. 543 - 547
