Masters, Kye-Simeon; Rauws, Tom R. M.; Yadav, Ashok K.; Herrebout, Wouter A.; Van Der Veken, Benjamin; Maes, Bert U. W.
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6315 - 6320
1: 6 h / 160 °C / Inert atmosphere; Neat (no solvent)
2: oxygen; copper (II) acetate monohydrate; 3,4,5-trifluoro-benzoic acid / dimethyl sulfoxide / 24 h / 120 °C
3: trans-1,2-cyclohexanediamine; copper (II) acetate monohydrate; caesium carbonate / dimethyl sulfoxide / 48 h / 120 °C
View Scheme
参考文献
Masters, Kye-Simeon; Rauws, Tom R. M.; Yadav, Ashok K.; Herrebout, Wouter A.; Van Der Veken, Benjamin; Maes, Bert U. W.
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6315 - 6320
1: diphenyl diselenide With hypophosphorous ether; glycerol in water
T=90°C; 0.5 h; Inert atmosphere;
2: alpha-chloropyridine in water
T=20°C; 2 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Thurow, Samuel; Webber, Rodrigo; Perin, Gelson; Lenardao, Eder J.; Alves, Diego
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3215 - 3218
