N,N-二甲基-1,3-二氨基丙烷合成路线 （共 206 条）
反应条件
1: 170 °C 2: lithium alanate; diethyl ether 3: ethanol View Scheme
参考文献
Rice et al.
Journal of the American Chemical Society, 1953 , vol. 75, p. 4911,4914
参考文献
Tosoh Corporation; KISO, Hiroyuki; SUZUKI, Takao; TAKAHASHI, Yoshihiro
Patent: EP2657237 A1, 2013 ;
Location in patent: Paragraph 0149; 0150 ;
参考文献
Chiti; Selleri
Farmaco, Edizione Scientifica, 1958 , vol. 13, p. 261,282
反应条件
in diethyl ether 2 h; Ambient temperature; Yield given;
参考文献
Williams,A.; Ibrahim,I.T.
Journal of the American Chemical Society, 1981 , vol. 103, p. 7090
反应条件
T=140°C; 12 h; Inert atmosphereSealed tube;
参考文献
Gogate, Priyanka N.; Ethirajan, Manivannan; Kurenova, Elena V.; Magis, Andrew T.; Pandey, Ravindra K.; Cance, William G.
European Journal of Medicinal Chemistry, 2014 , vol. 80, p. 154 - 156
参考文献
Reynaud,P. et al.
Chimica Therapeutica, 1971 , vol. 6, p. 25 - 41
反应条件
in iso-paraffin T=82.2122 - 93.3233°C; 14 - 16 h; Heating / reflux;
参考文献
CLEARWATER INTERNATIONAL, LLC; HARDING, Richard, Patrick
Patent: WO2004/43938 A1, 2004 ;
Location in patent: Page 4 ;
反应条件
in water Product distribution;
参考文献
Fuchslueger, Ulf
Analytical Chemistry, 1999 , vol. 71, # 13 p. 2324 - 2333
参考文献
Reynaud,P. et al.
Chimica Therapeutica, 1971 , vol. 6, p. 25 - 41
参考文献
Reynaud,P. et al.
Chimica Therapeutica, 1971 , vol. 6, p. 25 - 41
