N,N-二甲基-1,3-二氨基丙烷合成路线 (共 206 条)
参考文献
General Aniline Corp.
Patent: DE1139738 , 1963 ;
Chem.Abstr., 1963 , vol. 58, # 11375
反应条件
in chlorobenzene
T=125°C; 0.25 h; Neat (no solvent);
参考文献
DyStar Textilfarben GmbH and Co. Deutschland KG; Kao Corporation
Patent: EP1820826 A1, 2007 ;
Location in patent: Page/Page column 13 ;
参考文献
Du Pont de Nemours and Co.
Patent: US2701802 , 1953 ;
反应条件
triethylamine in dichloromethane
T=0 - 20°C; 12.33 h;
参考文献
DIONEX CORPORATION
Patent: WO2006/31717 A1, 2006 ;
Location in patent: Page/Page column 23-24 ;
参考文献
Patil, Sudhir; Mhatre, Dilip; D'Souza, Avila
Patent: US2006/182696 A1, 2006 ;
Location in patent: Page/Page column 4 ;
反应条件
1-methyl-piperazine; pyridine
参考文献
Petersen,H.J. et al.
Journal of Medicinal Chemistry, 1978 , vol. 21, p. 773 - 781
参考文献
Baitiche, Milad; Mahamoud, Abdallah; Benachour, Djaffar; Merbah, Meriem; Barbe, Jacques
Heterocyclic Communications, 2004 , vol. 10, # 4-5 p. 269 - 272
反应条件
sodium iodide; phenol
T=130°C; 1.5 h; Yield given;
参考文献
Yamato; Takeuchi; Hashigaki; Ikeda; Ming-Rong; Matsushima; Tsuruo; Tashiro; Tsukagoshi; Yamashita; Nakano
Journal of Medicinal Chemistry, 1989 , vol. 32, # 6 p. 1295 - 1300
反应条件
copper
T=180°C; unter Druck;
参考文献
Sargent; Small
Journal of Organic Chemistry, 1946 , vol. 11, p. 359,360, 361
反应条件
in ethylene glycol dimethyl ether
2 h; Heating;
参考文献
Shaw, John T.; Coffindaffer, Timothy W.; Stimmel, Julie B.; Lindley, Patricia M.
Journal of Heterocyclic Chemistry, 1982 , vol. 19, p. 357 - 361