N,N-二甲基-1,3-二氨基丙烷合成路线 (共 206 条)
反应条件
N,N,N',N,-tetramethylethylenediamine
Heating;
参考文献
Murdock,K.C. et al.
Journal of Medicinal Chemistry, 1979 , vol. 22, # 9 p. 1024 - 1030
反应条件
hydrogenchloride
T=180°C;
参考文献
Taylor
Journal of the American Chemical Society, 1952 , vol. 74, p. 1648
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Potter; Henshall
Journal of the Chemical Society, 1956 , p. 2000,2003
参考文献
Taylor
Journal of the American Chemical Society, 1952 , vol. 74, p. 1648
参考文献
Taylor
Journal of the American Chemical Society, 1952 , vol. 74, p. 1648
反应条件
(i) Et3N, benzene, (ii) LiAlH4; Multistep reaction;
参考文献
Powers; Dillingham; Bass
Journal of Pharmaceutical Sciences, 1975 , vol. 64, # 5 p. 883 - 885
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate in toluene
T=60 - 160°C; 2.33333 h; Microwave irradiation;
参考文献
Dahl, Troels; Tornoe, Christian W.; Bang-Andersen, Benny; Nielsen, Poul; Jorgensen, Morten
Angewandte Chemie - International Edition, 2008 , vol. 47, # 9 p. 1726 - 1728
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate in toluene
T=20 - 160°C;
参考文献
Dahl, Troels; Tornoe, Christian W.; Bang-Andersen, Benny; Nielsen, Poul; Jorgensen, Morten
Angewandte Chemie - International Edition, 2008 , vol. 47, # 9 p. 1726 - 1728
参考文献
Evonik Goldschmidt GmbH
Patent: US2009/54521 A1, 2009 ;
Location in patent: Page/Page column 5 ;
参考文献
Krapcho et al.
Journal of the American Chemical Society, 1955 , vol. 77, p. 3632
参考文献
Roe,A.M.; Reavill,D.R.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 527 - 530
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Budzikiewicz, Herbert; Vieth, Peter-Eric; Krueger, Uwe
Monatshefte fuer Chemie, 1981 , vol. 112, p. 825 - 840