N,N-二甲基-1,3-二氨基丙烷合成路线 （共 206 条）
参考文献
Limanov, V. E.; Epshtein, A. E.; Yakushkin, M. I.; Telegin, M. Yu.; Kotov, V. I.; et al.
Pharmaceutical Chemistry Journal, 1981 , vol. 15, # 2 p. 85 - 87
Khimiko-Farmatsevticheskii Zhurnal, 1981 , vol. 15, # 2 p. 28 - 30
反应条件
T=160 - 200°C; 9 - 11.8 h; Product distribution / selectivity;
参考文献
LION AKZO CO., LTD.
Patent: US2007/10680 A1, 2007 ;
Location in patent: Page/Page column 10-12 ;
反应条件
T=120 - 130°C; 24 h;
参考文献
Ngo, Thi Huong Viet; Damas, Christine; Naejus, Regine; Coudert, Robert
Journal of Fluorine Chemistry, 2010 , vol. 131, # 6 p. 704 - 708
反应条件
aluminum oxide; NAF T=160°C; 10 h; Inert atmosphere;
参考文献
Chu, Zonglin; Feng, Yujun
Synlett, 2009 , # 16 p. 2655 - 2658
反应条件
in N,N-dimethyl-formamide Ambient temperature;
参考文献
Guerrera; Salerno; Sarva; Siracusa; Lamartina; Caruso; Cutuli
Farmaco, 1992 , vol. 47, # 9 p. 1149 - 1160
参考文献
MERCK PATENT GMBH
Patent: WO2004/20398 A1, 2004 ;
Location in patent: Page 14 ;
反应条件
in ethylene glycol T=190°C; 16 h;
参考文献
Alekseeva; Bokanov; Granik
Pharmaceutical Chemistry Journal, 2002 , vol. 36, # 6 p. 318 - 323
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; tris-(dibenzylideneacetone)dipalladium(0); sodium t-butanolate in toluene T=60 - 160°C; 2.33333 h; Microwave irradiation;
参考文献
Dahl, Troels; Tornoe, Christian W.; Bang-Andersen, Benny; Nielsen, Poul; Jorgensen, Morten
Angewandte Chemie - International Edition, 2008 , vol. 47, # 9 p. 1726 - 1728
反应条件
PPA; phosphoric acid; acetic acid in water
参考文献
Chemische Fabrik Stockhausen and Cie.
Patent: US4237067 A1, 1980 ;
反应条件
T=80°C; P=975.098 Torr; Microwave irradiation;
参考文献
Krull, Matthias; Kayser, Christoph; Morschhaeuser, Roman; Ritter, Helmut; Schmitz, Sarah
Patent: US2010/32284 A1, 2010 ;
Location in patent: Page/Page column 7 ;
