N,N-二甲基-1,3-二氨基丙烷合成路线 （共 206 条）
反应条件
titanium(IV) isopropylate; di-n-octyltin oxide T=138 - 155°C; P=375.038 Torr; 2.5 h;
参考文献
ROeHM GMBH and CO. KG
Patent: WO2006/56366 A1, 2006 ;
Location in patent: Page/Page column 15-16 ;
反应条件
Candida antarctica lipase B Novozyme 435 in 1,4-dioxane T=30°C; Michael addition; 1 h; KineticsProduct distribution; Further Variations:ReagentsSolventsTemperatureseduct and reagent amount;
参考文献
Torre, Oliver; Gotor-Fernandez, Vicente; Alfonso, Ignacio; Garcia-Alles, Luis Fernando; Gotor, Vicente
Advanced Synthesis and Catalysis, 2005 , vol. 347, # 7-8 p. 1007 - 1014
反应条件
hydroquinone; acetonitrile
参考文献
Am.Cyanamid Co.
Patent: US2595907 , 1950 ;
反应条件
carbon monoxide; tetracarbonylnickel(0); toluene
参考文献
Rohm and Haas Co.
Patent: US2773063 , 1954 ;
反应条件
2: LiAlH4 View Scheme
参考文献
Roe,A.M.; Reavill,D.R.
Journal of the Chemical Society [Section] C: Organic, 1966 , p. 527 - 530
反应条件
in tetrahydrofuran T=-5 - 20°C;
参考文献
Tan, Hong; Xiao, Huining
Tetrahedron Letters, 2008 , vol. 49, # 11 p. 1759 - 1761
参考文献
Limanov, V. E.; Epshtein, A. E.; Yakushkin, M. I.; Telegin, M. Yu.; Kotov, V. I.; et al.
Pharmaceutical Chemistry Journal, 1981 , vol. 15, # 2 p. 85 - 87
Khimiko-Farmatsevticheskii Zhurnal, 1981 , vol. 15, # 2 p. 28 - 30
参考文献
General Aniline Corp.
Patent: DE1139738 , 1963 ;
Chem.Abstr., 1963 , vol. 58, # 11375
反应条件
T=120 - 130°C; 24 h;
参考文献
Ngo, Thi Huong Viet; Damas, Christine; Naejus, Regine; Coudert, Robert
Journal of Fluorine Chemistry, 2010 , vol. 131, # 6 p. 704 - 708
反应条件
1: ethanol / 24 h / Heating 2: H2 / 5percent Pd/C / ethanol View Scheme
参考文献
Kirrane, Thomas M.; Boyer, Stephen J.; Burke, Jennifer; Guo, Xin; Snow, Roger J.; Soleymanzadeh, Lida; Swinamer, Alan; Zhang, Yunlong; Madwed, Jeffery B.; Kashem, Mohammed; Kugler, Stanley; O'Neill, Margaret M.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 738 - 742
