N,N-二甲基-1,3-二氨基丙烷合成路线 （共 206 条）
反应条件
2: HCO2H 3: LiAlH4 / diethyl ether View Scheme
参考文献
Somin,I.N.
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 4 p. 128 - 133,122 - 125
参考文献
Sieger et al.
Journal of the American Pharmaceutical Association (1912-1977), 1958 , vol. 47, p. 734,738
反应条件
in water Product distribution;
参考文献
Fuchslueger, Ulf
Analytical Chemistry, 1999 , vol. 71, # 13 p. 2324 - 2333
反应条件
in ethanol 24 h; Heating;
参考文献
Shiseido Co., Ltd.
Patent: US6204264 B1, 2001 ;
参考文献
Kirrane, Thomas M.; Boyer, Stephen J.; Burke, Jennifer; Guo, Xin; Snow, Roger J.; Soleymanzadeh, Lida; Swinamer, Alan; Zhang, Yunlong; Madwed, Jeffery B.; Kashem, Mohammed; Kugler, Stanley; O'Neill, Margaret M.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 1 p. 738 - 742
反应条件
2: LiAlH4 / diethyl ether 4: LiAlH4 / diethyl ether View Scheme
参考文献
Somin,I.N.
Zhurnal Organicheskoi Khimii, 1968 , vol. 4, # 4 p. 128 - 133,122 - 125
反应条件
1: 91 percent / p-TsOH / toluene / 0.5 h / 115 °C / microwave irradiation 2: 97 percent / KI; K2CO3 / 2 h / 100 °C / microwave irradiation View Scheme
参考文献
Schmitz, Jens; Heller, Eberhard; Holzgrabe, Ulrike
Monatshefte fur Chemie, 2007 , vol. 138, # 2 p. 171 - 174
反应条件
1: 51 percent / 1) Trimethylamine, 2) acetic acid / CH2Cl2 / 1) 40 min, 2) 2 h. 2: 37 percent / toluene / 6 h / 111 °C View Scheme
参考文献
Katritzky; Burgess; Patel
Journal of Heterocyclic Chemistry, 1982 , vol. 19, # 4 p. 741 - 745
参考文献
Rav-acha, Ch.; Ringel, I.; Sarel, S.; Katzhendler, J.
Tetrahedron, 1988 , vol. 44, # 18 p. 5879 - 5892
反应条件
1: NAF; aluminum oxide / neat (no solvent) / 10 h / 155 - 160 °C / |Inert atmosphere 2: water; ethanol / 12 h / 79 °C View Scheme
参考文献
Feng, Dan; Zhang, Yongmin; Chen, Quansheng; Wang, Jiyu; Li, Bin; Feng, Yujun
Journal of Surfactants and Detergents, 2012 , vol. 15, # 5 p. 657 - 661
