N,N-二甲基-1,3-二氨基丙烷合成路线 （共 206 条）
反应条件
tri-ruthenium(0)dodecacarbonyl in 1,4-dioxane T=100°C; P=9880 Torr; 18 h;
参考文献
Zhou, Da-Yang; Yoneda, Eiji; Onitsuka, Kiyotaka; Takahashi, Shigetoshi
Chemical Communications, 2002 , # 23 p. 2868 - 2869
反应条件
T=200°C; also with methyl acrylate; var. temp. and reaction time; also in the presence of amidation catalysts; Product distribution;
参考文献
Shirshin, K.V.; Kazantsev, O.A.; Zil'berman, E.N.; Danov, S.M.; Salov, V.N.
J. Appl. Chem. USSR (Engl. Transl.), 1992 , vol. 65, # 6.2 p. 1379 - 1383,1148 - 1152
反应条件
hydrogen T=140°C; P=22502.3 Torr;
参考文献
Gerlach, Till; Funke, Frank; Benisch, Christoph; Melder, Johann-Peter
Patent: US2004/220428 A1, 2004 ;
Location in patent: Page 6 ;
反应条件
hydrogen T=100 - 200°C; P=0 - 15001.5 Torr; Product distribution / selectivity;
参考文献
BASF AKTIENGESELLSCHAFT
Patent: WO2006/82202 A1, 2006 ;
Location in patent: Page/Page column 3; 9 ;
反应条件
1: 78 percent / acetic acid / Heating 2: 87 percent 3: 56 percent / NBS / dioxane / 3 h / Ambient temperature View Scheme
参考文献
Brambilla; Disalle; Briatico; Mantegani; Temperilli
European Journal of Medicinal Chemistry, 1989 , vol. 24, # 4 p. 421 - 426
反应条件
in dimethyl sulfoxide T=90°C; var. temp., var. solv., Ea, ΔS(excit.); KineticsRate constantThermodynamic data;
参考文献
Hosseini, Mir Wais; Blacker, A. John; Lehn, Jean-Marie
Journal of the Chemical Society, Chemical Communications, 1988 , p. 596 - 598
反应条件
in dimethyl sulfoxide T=70°C; var. temp., var. solv., Ea, ΔS(excit.); KineticsRate constantThermodynamic data;
参考文献
Kunikowski, Antoni; Ledochowski, Andrzej
Polish Journal of Chemistry, 1983 , vol. 57, # 4/5/6 p. 435 - 445
反应条件
sodium hydroxide in ethanol; water
参考文献
Murphy, Michael A; Malachowski, Mitchell R
Patent: US2005/85555 A1, 2005 ;
US 20050085555 A1
反应条件
Product distribution;
参考文献
Fuchslueger, Ulf
Analytical Chemistry, 1999 , vol. 71, # 13 p. 2324 - 2333
反应条件
2 h; Heating; Yield given;
参考文献
Kusuma; Wilson; Boykin
Journal of Heterocyclic Chemistry, 1985 , vol. 22, # 5 p. 1229 - 1232
