sodium hydroxide; tetra(n-butyl)ammonium hydrogensulfate in water T=70°C; 48 h;
参考文献
Jacobus, David P.; Schiehser, Guy A.; Shieh, Hong-Ming; Jensen, Norman P.; Terpinski, Jacek
Patent: US2004/116428 A1, 2004 ;
Location in patent: Page 18 ;
1: 3-Methylbenzonitrile With ammonia; lithium; tert-butyl alcohol in tetrahydrofuran T=-35°C; 2: 1,3-dibromo-propane in tetrahydrofuran; ammonia cooling; Further stages.;
参考文献
Russian Chemical Bulletin, , vol. 55, # 6 p. 981 - 986