反应条件
water in diethyl ether; dichloromethane under Ar, addn. of a soln. of Sn compd. (ether) to a soln. (ether) of the amide at 0°C, colour changed from yellow to green, after 1 h cooling to -78°C, addn. of a soln. of BuLi (ether) and CH2Cl2, warming to room temp., pptn., hydrolysis; extd. (ether), organic layer washed (ether, aq. NaCl), dried (Na2SO4), evapn., TLC (silica gel);
参考文献
Nakadaira, Yasuhiro; Sato, Ryuji; Sakurai, Hideki
Journal of Organometallic Chemistry, 1992 , vol. 441, # 3 p. 411 - 417
