methyl iodide in tetrahydrofuran; hexane
addn. of BuLi-soln. in hexane to W-complex in THF, stirring for 1 h; react. under inert atmosphere; evapn. (vacuum), column chromy. (hexane), monitored by IR and NMR;
参考文献
Cervantes, Jorge; Vincenti, Steven P.; Kapoor, Ramesh N.; Pannell, Keith H.
Organometallics, 1989 , vol. 8, p. 744 - 748
methyl iodide in tetrahydrofuran; hexane
addn. of BuLi-soln. in hexane to W-complex in THF, stirring for 1 h; react. under inert atmosphere; evapn. (vacuum), column chromy. (elution with hexane), react. monitored by IR and NMR;
参考文献
Cervantes, Jorge; Vincenti, Steven P.; Kapoor, Ramesh N.; Pannell, Keith H.
Organometallics, 1989 , vol. 8, p. 744 - 748
