反应条件
in tetrahydrofuran N2-atmosphere; stirring (room temp., 40 min), Mn-compd. addn., stirring (-90 to -70°C, 3 h); evapn. (vac., -50 to -40°C), chromy. (alumina, -25°C, petroleum ether, petroleum ether / CH2Cl2 = 20 : 1, petroleum ether / CH2Cl2/ Et2O = 10 : 1 : 1), evapn. (vac.), recrystn. (petroleum ether / CH2Cl 2, -80°C); elem. anal.;
参考文献
Organometallics, , vol. 17, # 4 p. 600 - 606
