N-甲基-2-羟基乙胺合成路线 (共 285 条)
反应条件
tributyl(diethylamino)stannane Ambient temperature;
参考文献
Lown; Chauhan
Journal of Organic Chemistry, 1983 , vol. 48, # 22 p. 3901 - 3908
反应条件
triphenyl antimony oxide in methanol 1 h; Ambient temperature;
参考文献
Nomura, Ryoki; Kori, Masakuni; Matsuda, Haruo
Chemistry Letters, 1985 , p. 579 - 580
反应条件
potassium carbonate in benzene T=5°C; 2 h;
参考文献
Devillanova, Francesco A.; Verani, Gaetano
Journal of Heterocyclic Chemistry, 1980 , vol. 17, p. 571 - 573
反应条件
methanol; 2-hydroxy-N,N,N-trimethyl-ethanaminium T=32 - 48°C; P=110326 - 147102 Torr;
参考文献
Rohm and Haas Co.
Patent: US2793211 , 1954 ;
参考文献
de Benneville et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 772
反应条件
potassium carbonate in dimethyl sulfoxide a) RT, 5 d, b) 60 deg C, 5 h;
参考文献
Lupo, Donald; Ringsdorf, Helmut; Schuster, Andreas; Seitz, Markus
Journal of the American Chemical Society, 1994 , vol. 116, # 23 p. 10498 - 10506
反应条件
1: With titanium(IV) isopropylate in ethanol T=20°C; 6 h; Inert atmosphere; 2: With sodium tetrahydroborate in ethanol T=20°C; Inert atmosphereCooling with ice;
参考文献
Klein, Jan J.; Hecht, Stefan
Organic Letters, 2012 , vol. 14, # 1 p. 330 - 333
反应条件
tetrabutylammomium bromide; triethylamine in benzene 48 h; Heating;
参考文献
Afonso, Carlos A. M.; Lourenco, Nuno M. T.; De Rosatella, Andreia A.
Molecules, 2006 , vol. 11, # 1 p. 81 - 102
反应条件
1: With sodium hydrogencarbonate in tetrahydrofuran T=0 - 20°C; 2: With lithium aluminium tetrahydride in tetrahydrofuran T=0 - 20°C; Further stages.;
参考文献
Tayama, Eiji; Tanaka, Hiroyuki
Tetrahedron Letters, 2007 , vol. 48, # 24 p. 4183 - 4185
反应条件
triethylamine in acetonitrile T=0 - 20°C; 1.5 h;
参考文献
Baranyai, Zsolt; Rolla, Gabriele A.; Negri, Roberto; Forgacs, Attila; Giovenzana, Giovanni B.; Tei, Lorenzo
Chemistry - A European Journal, 2014 , vol. 20, # 10 p. 2933 - 2944