N-甲基-2-羟基乙胺合成路线 (共 285 条)
参考文献
Gruenenthal GmbH; FRANK, Robert; Christoph, Thomas; Lesch, Bernhard; Lee, Jeewoo
Patent: US2013/29961 A1, 2013 ;
Location in patent: Paragraph 0739 ;
反应条件
triethylamine in dichloromethane T=23°C; 3 h;
参考文献
Takahashi, Eiki; Hirano, Noriyuki; Nagahara, Takashi; Yoshikawa, Satoru; Momen, Shinobu; Yokokawa, Hiroshi; Hayashi, Ryoji
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 11 p. 3154 - 3156
反应条件
sodium acetate; palladium dichloride in ethylene glycol dimethyl ether T=80°C; P=2280 Torr;
参考文献
Journal of Organic Chemistry, , vol. 51, # 15 p. 2977 - 2981
反应条件
selenium; triethylamine in N,N-dimethyl-formamide 3 h;
参考文献
Journal of Organic Chemistry, , vol. 48, # 22 p. 3901 - 3908
反应条件
di(n-butyl)tin oxide in 1-methyl-pyrrolidin-2-one T=180°C; P=37503 Torr; 16 h;
参考文献
Synlett, , # 2 p. 307 - 309
反应条件
in chloroform 0.5 h; Ambient temperature;
参考文献
Synthesis, , # 12 p. 1032 - 1033
反应条件
1,3-dichloro-1,1,3,3-tetrabutyldistannoxane T=80°C; 1 h;
参考文献
Journal of Molecular Catalysis A: Chemical, , vol. 338, # 1-2 p. 33 - 43
反应条件
4-(N,N-dimethlyamino)pyridine in acetonitrile T=20°C; Condensation; cyclocondensation; 10 h; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 65, # 20 p. 6368 - 6380
反应条件
thionyl chloride anschliessend mit Chlorokohlensaeure-alkylester in wss. NaOH und Erhitzen des Reaktionsprodukts;
参考文献
Journal of the Chemical Society, , p. 4525
Journal of the Chemical Society, , p. 2836
反应条件
T=175 - 200°C; P=40452.9 Torr;
参考文献
Sasaki
Yuki Gosei Kagaku Kyokaishi, 1958 , vol. 16, p. 614,615,617
Chem.Abstr., 1959 , p. 3234