反应条件
in ethanol; 2-methoxy-ethanol byproducts: EtCl, Et2O, MeCHO; Electrochem. Process; anodic oxidation of W in EtOH in the presence of LiCl (110 V, 12 h), theson. left in contact with the atmosphere for 2 d, isoln. of the byprodu ct, addn. of MeOCH2CH2OH, heating to 60°C; evapn. (vac.), repeating the last procedure above twice, crystn. on layering the obtained liquor with hexane after 18 h; elem. anal.;
参考文献
Kessler, Vadim G.; Panov, Andrei N.; Turova, Nataliya Ya.; Starikova, Zoya A.; Yanovsky, Alexandr I.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1998 , # 1 p. 21 - 30
