反应条件
triphenylphosphine in 2-methoxy-ethanol Soln. of complex in 2-methoxyethanol was treated with an excess of PPh3, mixt. was heated at reflux for 4 h under inert atm.;; Ppt. was filtered. washed with a mixt. of Et2O/petroleum ether and dried in vac,;;
参考文献
Barral, M. C.; Jimenez-Aparicio, R.; Larrubia, M. J.; Royer, E. C.; Urbanos, F. A.
Inorganica Chimica Acta, 1991 , vol. 186, p. 239 - 242
