carbon monoxide in neat (no solvent) High Pressure; under dried N2; addn. of N-methylbenzimine at 25°C to a soln. of W-complex (CO-pressure: 50 atm); stirring for 2 d at room temp., then for 1-2 h at 80-100°C; vac.-evapn. until dryness; residue dissolved in petroleum ether/ether; chromy. (silica gel/petroleum ether/ether); recrystn. from petroleum ether; elem. anal.;
参考文献
Kron, Johanna; Schubert, Ulrich
Journal of Organometallic Chemistry, 1989 , vol. 373, p. 203 - 220
Eichinger, Peter C.H.; Bowie, John H.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 11 p. 1763 - 1768
