tetrahydrofuran; nitrogen T=-80°C; Hydrolysis.bei anschliessenden Hydrolyse und Dehydratisierung des erhaltenen Heptafluorbutyraldehyd-hydrats mit hilfe von Phosphor(V)-oxid;
参考文献
Henne; Francis
Journal of the American Chemical Society, 1953 , vol. 75, p. 992
in tetrahydrofuran reaction at -80°C, 23 hours and at -30°C, 20 hours; distillation over P2O5;;
参考文献
Henne; Francis
Journal of the American Chemical Society, 1953 , vol. 75, p. 992
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Gmelin Handbook: F: PerFHalOrg.4, 2.2.4, page 68 - 115