反应条件
hydrogenchloride; triphenylphosphine in ethanol byproducts: NH4Cl; according to Johnson, B. F. G., Segal, J. A., J. Chem. Soc., Dalton Trans., 1972, 1268; refluxing/stirring (15 min, CH2Cl2/MeOH 2:1 v/v, bubbling with HCl gas); concn. of mixt., pptn. on addn. of MeOH, CH2Cl2 and PPh3;
参考文献
Khan, M. Ishaque; Agarwala, U. C.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1989 , p. 1139 - 1142