反应条件
byproducts: KCl; soln. of 2 molar equiv. Fe complex in THF added dropwise to a soln. of Ga dimer at ambient temp. under N2 with stirring; stirred for an additional 2 h at room temp.; colour of the mixt. turned red, gray ppt. formed; filtered, evapd., redissolved in THF, overlayered with pentane at -30°C; crystals sepd. off; identified by elem. anal. and single crystalX-ray diffraction;
参考文献
Linti, Gerald; Li, Guangming; Pritzkow, Heinz
Journal of Organometallic Chemistry, 2001 , vol. 626, # 1-2 p. 82 - 91
