1-甲基-4-硝基-1H-咪唑-2-甲酰氯合成路线 (共 4 条)
反应条件
oxalyl dichloride in chloroform; acetonitrile Heating;
参考文献
Journal of Organic Chemistry, , vol. 52, # 16 p. 3493 - 3501
参考文献
Research Corporation Technologies, Inc.
Patent: US5273991 A1, 1993 ;
反应条件
1: 46.5 percent / conc. H2SO4, 100percent HNO3 / 0.83 h / 95 °C 2: 95 percent / NaOH / H2O / 0.25 h / Heating 3: oxalyl chloride / acetonitrile; CHCl3 / Heating View Scheme
参考文献
Krowicki, Krzysztof; Lown, J. William
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3493 - 3501
反应条件
1: 95 percent / NaOH / H2O / 0.25 h / Heating 2: oxalyl chloride / acetonitrile; CHCl3 / Heating View Scheme
参考文献
Krowicki, Krzysztof; Lown, J. William
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3493 - 3501