2,2'-联吡啶-4,4'-二甲醇合成路线 （共 14 条）
反应条件
sodium tetrahydroborate in ethanol Reflux;
参考文献
Tetrahedron Asymmetry, , vol. 24, # 8 p. 515 - 525
反应条件
sodium tetrahydroborate; ethanol Reflux;
参考文献
Chemical Communications, , # 48 p. 7545 - 7547
反应条件
1: 50 percent / aq. H2SO4; KMnO4 / 12 h / Heating 2: 99 percent / conc. H2SO4 / 60 h / Heating 3: 30 percent / NaBH4 / methanol / 60 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 18 p. 5919 - 5925
反应条件
1: 99 percent / conc. H2SO4 / 60 h / Heating 2: 30 percent / NaBH4 / methanol / 60 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 129, # 18 p. 5919 - 5925
反应条件
sodium hydroxide; sodium tetrahydroborate in methanol T=20°C; 1 h;
参考文献
European Journal of Inorganic Chemistry, , # 4 p. 1019 - 1029
反应条件
sodium hydroxide; water in methanol 3 h; Heating;
参考文献
Heterocycles, , vol. 56, # 1-2 p. 157 - 170
反应条件
sodium hydroxide in tetrahydrofuran; N,N-dimethyl-formamide Substitution;
参考文献
Tetrahedron Letters, , vol. 41, # 16 p. 2787 - 2789
反应条件
sodium hydroxide in tetrahydrofuran; N,N-dimethyl-formamide Substitution;
参考文献
Tetrahedron Letters, , vol. 41, # 16 p. 2787 - 2789
反应条件
1: BrF2CCF2Br; CsF / dimethylformamide / 2 h / 25 °C 2: dimethylformamide / 3 h / 50 °C 3: Na2CO3 / H2O; tetrahydrofuran / 10 h / reflux View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 16 p. 2787 - 2789
反应条件
1: 43.5 percent / acetic acid / 4 h / Heating 2: 44 percent / NaOH; water / methanol / 3 h / Heating View Scheme
参考文献
Heterocycles, , vol. 56, # 1-2 p. 157 - 170
