5-(羟甲基)吡啶-2(1H)-酮合成路线 (共 3 条)
反应条件
hydrogen; nickel monoaluminide in ethanol; ethyl acetate
反应条件
1: With lithium borohydride in tetrahydrofuran T=55°C; 5 h; Inert atmosphere; 2: With methanol; water in tetrahydrofuran T=20°C; 0.333333 h;
参考文献
WO2011/12622 A1, ;
Page/Page column 110 ;
WO 2011/012622 A1
反应条件
phosphorus pentachloride in chloroform; water; trichlorophosphate
参考文献
Lonza Ltd.
Patent: US6022974 A1, 2000 ;