1092383-57-7合成路线 （共 10 条）
反应条件
tris-(dibenzylideneacetone)dipalladium(0); sodium acetate in benzonitrile T=100°C; Heck reaction; 1 h; Microwave irradiation; stereoselective reaction;
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
反应条件
tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=25 - 150°C; Heck reaction; 0.0916667 h; Microwave irradiation;
参考文献
Amaral, Patricia A.; Gouault, Nicolas; Roch, Myriam Le; Eifler-Lima, Vera L.; David, Michele
Tetrahedron Letters, 2008 , vol. 49, # 47 p. 6607 - 6609
反应条件
1: [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate / 1 h / 80 °C / Microwave irradiation 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / Inert atmosphere; Reflux View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
反应条件
1: [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate / 1 h / 80 °C / Microwave irradiation 2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / Inert atmosphere; Reflux 3: 5 Pd(II)/C(eggshell); hydrogen / methanol / 1.5 h / 20 °C View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
反应条件
1: [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate / 1 h / 100 °C / Microwave irradiation 2: palladium 10 on activated carbon; hydrogen / methanol / 12 h / 20 °C View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
反应条件
tris-(dibenzylideneacetone)dipalladium(0); sodium acetate in benzonitrile T=100°C; Heck reaction; 1 h; Microwave irradiation; stereoselective reaction;
参考文献
Organic Letters, , vol. 11, # 16 p. 3642 - 3645
反应条件
tetrakis(triphenylphosphine) palladium(0); N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide T=25 - 150°C; Heck reaction; 0.0916667 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 49, # 47 p. 6607 - 6609
反应条件
1: [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate / 1 h / 100 °C / Microwave irradiation 2: palladium 10 on activated carbon; hydrogen / methanol / 12 h / 20 °C View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
反应条件
1: [Pd2(dibenzylideneacetone)3]*dibenzylideneacetone; sodium acetate / 0.5 h / 80 °C / Microwave irradiation
2: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / Inert atmosphere; Reflux
3: 5 Pd(II)/C(eggshell); hydrogen / methanol / 1.5 h / 20 °C
View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
反应条件
1.1: sodium acetate; palladium diacetate / acetonitrile / 0.17 h
1.2: 3 h
2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 2 h / Inert atmosphere; Reflux
View Scheme
参考文献
Soldi, Cristian; Moro, Angelica V.; Pizzolatti, Moacir G.; Correia, Carlos R. D.
European Journal of Organic Chemistry, 2012 , # 19 p. 3607 - 3616
